4UW0
Low resolution structure of WbdD with C-terminal bundle ordered to residue 505
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Wavelength(s) | 0.91730 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 181.290, 181.290, 181.290 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 128.190 - 3.870 |
| R-factor | 0.27097 |
| Rwork | 0.268 |
| R-free | 0.34096 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.301 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 128.200 |
| High resolution limit [Å] | 3.870 |
| Rmerge | 0.070 |
| Number of reflections | 9283 |
| <I/σ(I)> | 11.6 |
| Completeness [%] | 98.6 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
