4UVK

Cohesin subunit Scc3 from Z. rouxii, 88-1035

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS
Spacegroup name	P 21 21 21
Unit cell lengths	73.372, 109.176, 159.029
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.347 - 2.600
R-factor	0.1901
Rwork	0.187
R-free	0.24500
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.015
RMSD bond angle	1.549
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.080	0.400
Number of reflections	39907
<I/σ(I)>	14.3	3.5
Completeness [%]	99.7	99.9
Redundancy	3.7	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1