4UTI
XenA - oxidized - Y183F variant in complex with coumarin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY |
Synchrotron site | BESSY |
Beamline | BL14-1 |
Temperature [K] | 100 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 57.870, 83.397, 156.366 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.729 - 1.099 |
R-factor | 0.1251 |
Rwork | 0.125 |
R-free | 0.14100 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.382 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.730 |
High resolution limit [Å] | 1.100 |
Rmerge | 0.060 |
Number of reflections | 151912 |
<I/σ(I)> | 2.56 |
Completeness [%] | 99.0 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |