Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 57.477, 83.218, 156.162 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.241 - 1.250 |
R-factor | 0.1372 |
Rwork | 0.136 |
R-free | 0.16420 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.266 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.240 |
High resolution limit [Å] | 1.250 |
Rmerge | 0.060 |
Number of reflections | 103079 |
<I/σ(I)> | 14.01 |
Completeness [%] | 99.6 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |