4USM
WcbL complex with glycerol bound to sugar site
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-09-20 |
Detector | ADSC CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 101.050, 115.890, 167.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 76.160 - 1.820 |
R-factor | 0.19187 |
Rwork | 0.190 |
R-free | 0.22872 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.339 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | SHELX |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.160 | 1.870 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.080 | 0.800 |
Number of reflections | 87041 | |
<I/σ(I)> | 15.4 | 1.9 |
Completeness [%] | 99.1 | 93.8 |
Redundancy | 7.2 | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.5 M NACL, 10 MM HEPES PH 7 |