4UNV
Covalent dimer of lambda variable domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-05-03 |
Detector | RIGAKU CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 37.417, 60.212, 79.417 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.110 - 1.600 |
R-factor | 0.19612 |
Rwork | 0.193 |
R-free | 0.25793 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mcg |
RMSD bond length | 0.018 |
RMSD bond angle | 1.962 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.060 | 0.400 |
Number of reflections | 11350 | |
<I/σ(I)> | 39 | 4.2 |
Completeness [%] | 98.0 | 86 |
Redundancy | 7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 0.1M CH3COONA PH4.6, 2M (NH4)2SO4 |