4UNU
MCG - a dimer of lambda variable domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-10-26 |
Detector | DECTRIS PILATUS 6M-F |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.340, 34.120, 63.180 |
Unit cell angles | 90.00, 104.94, 90.00 |
Refinement procedure
Resolution | 39.940 - 0.950 |
R-factor | 0.10846 |
Rwork | 0.107 |
R-free | 0.12996 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mcg |
RMSD bond length | 0.026 |
RMSD bond angle | 2.291 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 0.970 |
High resolution limit [Å] | 0.950 | 0.950 |
Rmerge | 0.070 | 0.700 |
Number of reflections | 89567 | |
<I/σ(I)> | 21 | 1.9 |
Completeness [%] | 88.0 | 34 |
Redundancy | 12 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 2M NACL, 2M (NH4)2SO4, pH 8 |