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4UNH

Human insulin B26Gly mutant crystal structure

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID29
Synchrotron siteESRF
BeamlineID29
Temperature [K]100
Detector technologyCCD
Collection date2010-02-06
DetectorADSC CCD
Spacegroup nameI 41 2 2
Unit cell lengths45.524, 45.524, 117.411
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution42.450 - 2.750
R-factor0.24248
Rwork0.237
R-free0.35516
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1mso
RMSD bond length0.012
RMSD bond angle1.518
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0033)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.5202.800
High resolution limit [Å]2.7502.750
Rmerge0.1400.340
Number of reflections1812
<I/σ(I)>123
Completeness [%]94.059.3
Redundancy12.79.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
140.08 M NA2SO4, PH 4.0, CP = 5 MG/ML

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