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4UNG

Human insulin B26Asn mutant crystal structure

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I02
Synchrotron siteDiamond
BeamlineI02
Temperature [K]100
Detector technologyCCD
Collection date2010-02-04
DetectorADSC CCD
Spacegroup nameP 41 21 2
Unit cell lengths45.630, 45.630, 117.720
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution36.060 - 1.810
R-factor0.17594
Rwork0.174
R-free0.21992
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1mso
RMSD bond length0.019
RMSD bond angle1.782
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0033)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.6301.850
High resolution limit [Å]1.8101.810
Rmerge0.1100.820
Number of reflections12092
<I/σ(I)>19.14.2
Completeness [%]99.699.6
Redundancy14.215.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
140.035 M (NH4)2SO4, PH 4.0, CP = 5 MG/ML

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