4UNB
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA AT 6 DAYS INCUBATION IN 5MM MN (STATE 5)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 107.128, 70.666, 107.375 |
Unit cell angles | 90.00, 119.62, 90.00 |
Refinement procedure
Resolution | 46.564 - 2.550 |
R-factor | 0.1794 |
Rwork | 0.177 |
R-free | 0.22140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs8 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.167 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.670 | 2.690 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.050 | 0.540 |
Number of reflections | 44171 | |
<I/σ(I)> | 17.2 | 2.8 |
Completeness [%] | 96.6 | 94.8 |
Redundancy | 4.8 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | PH 6 |