4UN7
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA BEFORE INCUBATION IN 5MM MN (STATE 1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 106.570, 70.347, 106.601 |
Unit cell angles | 90.00, 119.89, 90.00 |
Refinement procedure
Resolution | 46.195 - 2.700 |
R-factor | 0.1802 |
Rwork | 0.177 |
R-free | 0.23190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs7 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.192 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.210 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.070 | 0.640 |
Number of reflections | 37832 | |
<I/σ(I)> | 12.5 | 2 |
Completeness [%] | 99.7 | 99.5 |
Redundancy | 4.6 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6 |