4UMP
Structure of MELK in complex with inhibitors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-05-02 |
Detector | RIGAKU IMAGE PLATE RAXIS |
Spacegroup name | P 1 |
Unit cell lengths | 65.822, 74.968, 77.088 |
Unit cell angles | 86.47, 70.06, 89.94 |
Refinement procedure
Resolution | 50.380 - 2.300 |
R-factor | 0.2378 |
Rwork | 0.235 |
R-free | 0.29100 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 0.940 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.070 |
Number of reflections | 61286 |
<I/σ(I)> | 5.7 |
Completeness [%] | 95.8 |
Redundancy | 1.95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |