4UJ7
Structure of the S-layer protein SbsC, domains 5-6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.096, 43.753, 49.715 |
| Unit cell angles | 90.00, 103.78, 90.00 |
Refinement procedure
| Resolution | 48.280 - 1.540 |
| R-factor | 0.19121 |
| Rwork | 0.190 |
| R-free | 0.21665 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4iuc |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.242 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.300 | 1.640 |
| High resolution limit [Å] | 1.540 | 1.540 |
| Rmerge | 0.040 | 0.290 |
| Number of reflections | 30189 | |
| <I/σ(I)> | 15.7 | 3 |
| Completeness [%] | 98.8 | 95.7 |
| Redundancy | 3.4 | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
