4UHP
Crystal structure of the pyocin AP41 DNase-Immunity complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-07-16 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 |
Unit cell lengths | 36.604, 75.627, 83.171 |
Unit cell angles | 79.19, 78.05, 77.00 |
Refinement procedure
Resolution | 40.236 - 2.000 |
R-factor | 0.1882 |
Rwork | 0.186 |
R-free | 0.23470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bx1 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.667 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.240 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.180 | 0.940 |
Number of reflections | 55279 | |
<I/σ(I)> | 4.7 | 2.7 |
Completeness [%] | 97.2 | 96.2 |
Redundancy | 1.8 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 40% JEFFAMINE D2000, 0.1 M HEPES PH 6.5 |