4UDJ
Crystal structure of b-1,4-mannopyranosyl-chitobiose phosphorylase at 1.60 Angstrom in complex with beta-D-mannopyranose and inorganic phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-09-26 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 83.880, 140.840, 168.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 108.130 - 1.940 |
R-factor | 0.15173 |
Rwork | 0.150 |
R-free | 0.19333 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4udi |
RMSD bond length | 0.018 |
RMSD bond angle | 1.853 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.000 | 2.040 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.160 | 0.590 |
Number of reflections | 148390 | |
<I/σ(I)> | 4 | 1.2 |
Completeness [%] | 99.7 | 99.5 |
Redundancy | 8.2 | 7.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | PROTEIN WAS CRYSTALLIZED FROM 17.5% PEG 3350, 200 MM NH4CL, pH 7.0 |