Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4UB1

DNA polymerase beta product complex with a templating adenine and 8-oxodGMP, 90 s

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-BM
Synchrotron siteAPS
Beamline22-BM
Temperature [K]100
Detector technologyCCD
Collection date2013-06-27
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths55.131, 80.800, 55.462
Unit cell angles90.00, 109.58, 90.00
Refinement procedure
Resolution31.962 - 2.341
R-factor0.2278
Rwork0.222
R-free0.27720
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3isb
RMSD bond length0.010
RMSD bond angle1.061
Refinement softwarePHENIX ((phenix.refine: 1.7_650))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.390
High resolution limit [Å]2.3412.341
Rmerge0.0520.334
Number of reflections34952
<I/σ(I)>24.32.3
Completeness [%]97.377
Redundancy3.52.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP829150 mM imidazole, 350 mM sodium chloride, 17% PEG3350, pH 8.0

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon