4U76
HsMetAP (F309M) holo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-02-27 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.067, 77.469, 46.990 |
Unit cell angles | 90.00, 92.43, 90.00 |
Refinement procedure
Resolution | 18.720 - 1.870 |
R-factor | 0.18 |
Rwork | 0.177 |
R-free | 0.22300 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.953 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.870 |
Number of reflections | 26625 |
<I/σ(I)> | 3.1 |
Completeness [%] | 99.6 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 15% PEGMME, 100mM HEPES PH 6 |