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4U76

HsMetAP (F309M) holo form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2014-02-27
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.54
Spacegroup nameP 1 21 1
Unit cell lengths47.067, 77.469, 46.990
Unit cell angles90.00, 92.43, 90.00
Refinement procedure
Resolution18.720 - 1.870
R-factor0.18
Rwork0.177
R-free0.22300
RMSD bond length0.019
RMSD bond angle1.953
Refinement softwareREFMAC (5.7.0029)
Data quality characteristics
 Overall
Low resolution limit [Å]20.000
High resolution limit [Å]1.870
Number of reflections26625
<I/σ(I)>3.1
Completeness [%]99.6
Redundancy3.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP629815% PEGMME, 100mM HEPES PH 6

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