4U6J
HsMetAP in complex with methionine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-03-11 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.446, 77.340, 48.440 |
Unit cell angles | 90.00, 90.93, 90.00 |
Refinement procedure
Resolution | 18.530 - 1.560 |
R-factor | 0.127 |
Rwork | 0.125 |
R-free | 0.17600 |
RMSD bond length | 0.021 |
RMSD bond angle | 2.057 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.930 |
High resolution limit [Å] | 1.560 |
Number of reflections | 48263 |
<I/σ(I)> | 4.8 |
Completeness [%] | 97.0 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 15% PEG MME , 100mM HEPES PH6.0 , |