4U65
Structure of the periplasmic output domain of the Legionella pneumophila LapD ortholog CdgS9 in complex with Pseudomonas fluorescens LapG
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-05-01 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.976 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 75.854, 73.674, 88.223 |
| Unit cell angles | 90.00, 92.88, 90.00 |
Refinement procedure
| Resolution | 44.056 - 2.100 |
| R-factor | 0.1714 |
| Rwork | 0.170 |
| R-free | 0.21120 |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.641 |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.060 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 55783 |
| <I/σ(I)> | 12.4 |
| Completeness [%] | 97.7 |
| Redundancy | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 0.1 M Bis-Tris (pH=6.0) and 0.1 M magnesium formate |
