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4U55

Crystal structure of Cryptopleurine bound to the yeast 80S ribosome

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyPIXEL
Collection date2013-07-01
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths435.150, 287.070, 303.240
Unit cell angles90.00, 98.87, 90.00
Refinement procedure
Resolution99.870 - 3.200
R-factor0.1949
Rwork0.194
R-free0.24600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3U5B 3U5C 3U5D 3U5E 3U5F 3U5G 3U5H 3U5I
RMSD bond length0.013
RMSD bond angle1.650
Data reduction softwareXDS
Data scaling softwareXSCALE
Refinement softwarePHENIX ((phenix.refine: dev_1702))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]99.8703.300
High resolution limit [Å]3.20050.0003.200
Rmerge0.3670.0512.664
Rmeas0.3810.0592.807
Total number of observations15126527
Number of reflections1206041287106176
<I/σ(I)>8.0915.891.02
Completeness [%]100.082100
Redundancy9.71
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5277PEG 20K, KSCN, Mg Acetate, Tris-Acetate, Glycerol, Spermidine

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