4U4Y
Crystal structure of Pactamycin bound to the yeast 80S ribosome
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 436.920, 288.520, 305.750 |
Unit cell angles | 90.00, 99.04, 90.00 |
Refinement procedure
Resolution | 267.960 - 3.200 |
R-factor | 0.1939 |
Rwork | 0.193 |
R-free | 0.24530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3U5B 3U5C 3U5D 3U5E 3U5F 3U5G 3U5H 3U5I |
RMSD bond length | 0.013 |
RMSD bond angle | 1.660 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX ((phenix.refine: dev_1702)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 267.960 | 3.300 | |
High resolution limit [Å] | 3.200 | 200.000 | 3.200 |
Rmerge | 0.393 | 0.876 | 2.465 |
Rmeas | 0.404 | 0.971 | 2.637 |
Total number of observations | 21800731 | ||
Number of reflections | 1226463 | 5 | 107866 |
<I/σ(I)> | 8.71 | 2.7 | 0.86 |
Completeness [%] | 100.0 | 71.4 | 100 |
Redundancy | 7.71 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | PEG 20K, KSCN, Mg Acetate, Tris-Acetate, Glycerol, Spermidine |