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4U4Q

Crystal structure of Homoharringtonine bound to the yeast 80S ribosome

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyPIXEL
Collection date2013-07-01
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths436.250, 286.920, 303.840
Unit cell angles90.00, 98.90, 90.00
Refinement procedure
Resolution49.690 - 3.000
R-factor0.2088
Rwork0.208
R-free0.25460
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3U5B 3U5C 3U5D 3U5E 3U5F 3U5G 3U5H 3U5I
RMSD bond length0.012
RMSD bond angle1.616
Data reduction softwareXDS
Data scaling softwareXSCALE
Refinement softwarePHENIX ((phenix.refine: dev_1702))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]49.6903.100
High resolution limit [Å]3.00040.0003.000
Rmerge0.3410.0623.527
Rmeas0.3610.0723.725
Total number of observations13621629
Number of reflections1451516280134798
<I/σ(I)>7.1311.840.88
Completeness [%]98.841.298.2
Redundancy9.37
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5277PEG 20K, KSCN, Mg Acetate, Tris-Acetate, Glycerol, Spermidine

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