4U4Q

Crystal structure of Homoharringtonine bound to the yeast 80S ribosome

This is a large structure.

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (3 Å)

Cell axes436.250286.920303.840
Cell angles90.0098.9090.00
SpacegroupP 1 21 1
Resolution limits49.69 - 3.00
the highest resolution shell value3.034 - 3.000
R-factor0.2088
R-work0.20790
the highest resolution shell value0.336
R-free0.25460
the highest resolution shell value0.375
RMSD bond length0.012
RMSD bond angle1.616

Data Collection Statistics

Resolution limits49.69 - 3.00
the highest resolution shell value -
Number of reflections1451516
Rmerge_l_obs0.341
the highest resolution shell value3.527
Completeness98.8
Redundancy9.37
I/sigma(I)-3

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP7.5277

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*