4U4I
Megavirus chilensis superoxide dismutase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2012-10-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 70.626, 70.626, 117.426 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.040 - 2.200 |
R-factor | 0.1897 |
Rwork | 0.186 |
R-free | 0.22640 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.139 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.140 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.110 | 0.800 |
Number of reflections | 15785 | |
<I/σ(I)> | 6.3 | 1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 14.9 | 15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M sodium acetate buffer, 20%(w/v) PEG 4000, 20%(v/v) MPD |