4U2J
N-terminal domain of C. Reinhardtii SAS-6 homolog bld12p variant Q93E F145W (NN27)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-07 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.150, 97.000, 142.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 80.241 - 2.000 |
R-factor | 0.1938 |
Rwork | 0.191 |
R-free | 0.23970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.769 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.241 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 1.116 | |
Number of reflections | 38651 | |
<I/σ(I)> | 15.66 | 2.14 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.5 | 293 | PEG3350, MES-NaOH |