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4U21

GluA2flip sLBD complexed with FW and (R,R)-2b crystal form E

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.2
Synchrotron siteALS
Beamline5.0.2
Temperature [K]100
Detector technologyCCD
Collection date2013-01-02
DetectorADSC QUANTUM 315r
Wavelength(s)1
Spacegroup nameP 21 21 2
Unit cell lengths97.290, 121.320, 47.740
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution45.150 - 1.391
R-factor0.1834
Rwork0.183
R-free0.19820
RMSD bond length0.006
RMSD bond angle1.148
Data reduction softwareXDS
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 Overall
Low resolution limit [Å]45.150
High resolution limit [Å]1.390
Number of reflections110875
<I/σ(I)>18.2
Completeness [%]97.2
Redundancy3.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP293phosphate-citrate, pH 4.2, 0.2 M Li sulfate, 20% PEG1K

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