4U1Z

GluA2flip sLBD complexed with kainate and (R,R)-2b crystal form D

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	CCD
Collection date	2013-01-02
Detector	ADSC QUANTUM 315r
Wavelength(s)	1
Spacegroup name	P 21 21 2
Unit cell lengths	64.040, 90.610, 48.350
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.297 - 1.940
R-factor	0.169
Rwork	0.167
R-free	0.20770
RMSD bond length	0.009
RMSD bond angle	1.304
Data reduction software	XDS
Refinement software	PHENIX ((phenix.refine: 1.8.1_1168))

Data quality characteristics

	Overall
Low resolution limit [Å]	52.300
High resolution limit [Å]	1.940
Number of reflections	20910
<I/σ(I)>	12.6
Completeness [%]	97.4
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M Na acetate, pH 4.5, 25% PEG3350