4TZU
Crystal Structure of Murine Cereblon in Complex with Pomalidomide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-08-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00 |
Spacegroup name | I 2 3 |
Unit cell lengths | 143.340, 143.340, 143.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.1979 |
Rwork | 0.196 |
R-free | 0.23920 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.710 |
Data scaling software | SCALA (3.3.20) |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 101.357 | 41.379 | 2.110 |
High resolution limit [Å] | 2.000 | 6.320 | 2.000 |
Rmerge | 0.096 | 0.204 | |
Rmeas | 0.090 | ||
Rpim | 0.050 | 0.066 | 0.134 |
Total number of observations | 88108 | 2865 | 12968 |
Number of reflections | 30305 | ||
<I/σ(I)> | 10.1 | 14.3 | 5.4 |
Completeness [%] | 92.3 | 86.7 | 92.4 |
Redundancy | 2.9 | 3.1 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 100mM Sodium Acetate pH5, 600-800mM Ammonium Sulfate. |