4TYS
Crystal structure of Canavalia maritima lectin (ConM) complexed with a dinucleotide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LNLS BEAMLINE W01B-MX2 |
Synchrotron site | LNLS |
Beamline | W01B-MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-08-15 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.42 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 140.690, 140.570, 199.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.290 - 3.250 |
R-factor | 0.21859 |
Rwork | 0.216 |
R-free | 0.26706 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.939 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.290 |
High resolution limit [Å] | 3.250 |
Number of reflections | 31390 |
<I/σ(I)> | 5.4 |
Completeness [%] | 99.3 |
Redundancy | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2 M Magnesium formate dehydrate |