4TYS
Crystal structure of Canavalia maritima lectin (ConM) complexed with a dinucleotide
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LNLS BEAMLINE W01B-MX2 |
| Synchrotron site | LNLS |
| Beamline | W01B-MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-08-15 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.42 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 140.690, 140.570, 199.020 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.290 - 3.250 |
| R-factor | 0.21859 |
| Rwork | 0.216 |
| R-free | 0.26706 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.939 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 38.290 |
| High resolution limit [Å] | 3.250 |
| Number of reflections | 31390 |
| <I/σ(I)> | 5.4 |
| Completeness [%] | 99.3 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2 M Magnesium formate dehydrate |
