4TXA

Crystal structure of N-terminus of Roquin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2011-07-28
Detector	ADSC QUANTUM 210r
Wavelength(s)	1.265102
Spacegroup name	C 1 2 1
Unit cell lengths	142.804, 80.191, 54.858
Unit cell angles	90.00, 111.06, 90.00

Refinement procedure

Resolution	37.830 - 2.750
R-factor	0.2201
Rwork	0.218
R-free	0.25530
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.966
Refinement software	PHENIX ((phenix.refine: 1.8.2_1309))

Data quality characteristics

	Overall
Low resolution limit [Å]	68.710
High resolution limit [Å]	2.750
Number of reflections	14921
<I/σ(I)>	13.9
Completeness [%]	98.8
Redundancy	7.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9.5	293	7-20% PEG 8000, 0.1M CHES