4TWM
Crystal structure of dioscorin from Dioscorea japonica
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2011-02-06 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1.0000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 83.470, 156.770, 83.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.600 - 2.110 |
R-factor | 0.21236 |
Rwork | 0.209 |
R-free | 0.27162 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.838 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.110 |
Number of reflections | 31706 |
<I/σ(I)> | 39.3 |
Completeness [%] | 99.3 |
Redundancy | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 10 | 278 | CAPS, lithium sulfate, ammonium sulfate |