Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4TWB

Sulfolobus solfataricus ribose-phosphate pyrophosphokinase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsMAX II BEAMLINE I911-2
Synchrotron siteMAX II
BeamlineI911-2
Temperature [K]120
Detector technologyCCD
Collection date2010-01-01
DetectorMARRESEARCH
Wavelength(s)1.03908
Spacegroup nameP 1 21 1
Unit cell lengths80.217, 92.846, 138.338
Unit cell angles90.00, 90.91, 90.00
Refinement procedure
Resolution19.984 - 2.802
R-factor0.2361
Rwork0.235
R-free0.26470
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1u9y
RMSD bond length0.009
RMSD bond angle1.306
Data scaling softwareSCALEPACK
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.900
High resolution limit [Å]2.8002.800
Rmerge0.0890.590
Number of reflections48432
<I/σ(I)>142.4
Completeness [%]97.998.1
Redundancy4.14
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION5293Protein: 12.7 mg/mL 50 mM Tris/HCl pH 7.6 10 mM AMP 10 mM ribose 5-phosphate Buffer: 0.2 M diammonium citrate pH 5.0 Precipitant: 14 % PEG10000

223166

PDB entries from 2024-07-31

PDB statisticsPDBj update infoContact PDBjnumon