4TTZ
N-terminal domain of C. Reinhardtii SAS-6 homolog bld12p variant G94E F145W Q147K (NN26)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-07 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 96.510, 40.110, 142.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.245 - 2.500 |
R-factor | 0.2094 |
Rwork | 0.207 |
R-free | 0.25020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3q0y |
RMSD bond length | 0.002 |
RMSD bond angle | 0.516 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.250 | 2.560 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 1.123 | |
Number of reflections | 19737 | |
<I/σ(I)> | 23.94 | 2.66 |
Completeness [%] | 99.1 | 87.9 |
Redundancy | 14.1 | 11.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6 | 293 | PEG3350, MES-NaOH |