4TT0
Crystal structure of fragment 1600-1733 of HSV1 UL36 in the presence of 1M potassium iodide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-11 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.907450 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 110.939, 110.939, 154.930 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.038 - 2.599 |
R-factor | 0.1905 |
Rwork | 0.188 |
R-free | 0.24200 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.031 |
Data reduction software | XDS |
Phasing software | SHELXDE |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.038 |
High resolution limit [Å] | 2.599 |
Number of reflections | 32816 |
<I/σ(I)> | 14.5 |
Completeness [%] | 100.0 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 100 mM Hepes, 2M ammonium formate |