Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4TS6

Crystal structure of the RIM C2A domain from Drosophila.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2012-09-15
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.999
Spacegroup nameP 21 21 21
Unit cell lengths32.080, 38.700, 131.370
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution65.680 - 1.920
R-factor0.186
Rwork0.184
R-free0.21820
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2bwq
RMSD bond length0.007
RMSD bond angle1.190
Data reduction softwareXDS
Data scaling softwareAimless (3.11)
Phasing softwareMrBUMP
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]65.6801.970
High resolution limit [Å]1.9208.5901.920
Rmerge0.0570.0250.643
Rmeas0.0660.0290.751
Total number of observations90891
Number of reflections131882691756
<I/σ(I)>12.3928.681.97
Completeness [%]99.695.799.6
Redundancy6.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2770.2 M tri-lithium citrate, 20% w/v PEG 3350

227561

PDB entries from 2024-11-20

PDB statisticsPDBj update infoContact PDBjnumon