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4TS6

Crystal structure of the RIM C2A domain from Drosophila.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2012-09-15
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.999
Spacegroup nameP 21 21 21
Unit cell lengths32.080, 38.700, 131.370
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution65.680 - 1.920
R-factor0.186
Rwork0.184
R-free0.21820
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2bwq
RMSD bond length0.007
RMSD bond angle1.190
Data reduction softwareXDS
Data scaling softwareAimless (3.11)
Phasing softwareMrBUMP
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]65.6801.970
High resolution limit [Å]1.9208.5901.920
Rmerge0.0570.0250.643
Rmeas0.0660.0290.751
Total number of observations90891
Number of reflections131882691756
<I/σ(I)>12.3928.681.97
Completeness [%]99.695.799.6
Redundancy6.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2770.2 M tri-lithium citrate, 20% w/v PEG 3350

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