Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NW12A |
| Temperature [K] | 193 |
| Detector technology | CCD |
| Collection date | 2012-11-06 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 74.028, 74.028, 101.950 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.000 - 2.452 |
| R-factor | 0.2015 |
| Rwork | 0.199 |
| R-free | 0.25030 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.190 |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 30.000 | 30.000 | 2.490 |
| High resolution limit [Å] | 2.450 | 6.630 | 2.450 |
| Rmerge | 0.092 | 0.042 | 0.697 |
| Total number of observations | 69357 | ||
| Number of reflections | 12263 | ||
| <I/σ(I)> | 12.3 | ||
| Completeness [%] | 99.8 | 97.2 | 100 |
| Redundancy | 5.7 | 5 | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 0.1M HEPES, 0.2M Li2SO4, 20% (w/v) PEG3350 |
