4TRC
Sulfolobus solfataricus adenine phosphoribosyltransferase with adenine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 122 |
Detector technology | AREA DETECTOR |
Collection date | 2011-04-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.03911 |
Spacegroup name | P 61 |
Unit cell lengths | 137.200, 137.200, 53.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.705 - 2.400 |
R-factor | 0.2022 |
Rwork | 0.200 |
R-free | 0.24160 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.982 |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.400 |
Number of reflections | 22808 |
<I/σ(I)> | 28.26 |
Completeness [%] | 99.6 |
Redundancy | 13.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Protein 8.9 mg/mL 25 mM TRIS pH 7.6 0.1 mM EDTA 5 mM adenine Buffer 0.1 M phosphate-citrate pH 4.2 Precipitant 20 % PEG1000 0.2 M Li2SO4 |