4TQD

Crystal Structure of the C-terminal domain of IFRS bound with 3-iodo-L-Phe and ATP

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-04-14
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.9789
Spacegroup name	P 64
格子定数 [Å]	104.700, 104.700, 70.660
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	42.064 - 2.143
R因子	0.1589
Rwork	0.155
R-free	0.19250
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2zim
結合長の平均二乗偏差(RMSD) [Å]	0.014
結合角の平均二乗偏差(RMSD) [度]	1.450
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Quality characteristics

	Overall
分解能 [Å] (低)	42.064
分解能 [Å] (高)	2.140
独立反射数	24274
<I/σ(I)>	34.24
完全性 [%]	99.8
冗長性	20

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, SITTING DROP		298	Hepes, MgCl2, PEG3350