4TQ5
Structure of a UbiA homolog from Archaeoglobus fulgidus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-07-14 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97800 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 61.922, 61.922, 248.752 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.244 - 3.202 |
R-factor | 0.2548 |
Rwork | 0.251 |
R-free | 0.28860 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.952 |
Data reduction software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.260 |
High resolution limit [Å] | 3.200 | 8.670 | 3.200 |
Rmerge | 0.128 | 0.030 | |
Total number of observations | 197115 | ||
Number of reflections | 9401 | ||
<I/σ(I)> | 4.9 | ||
Completeness [%] | 99.9 | 100 | 98.7 |
Redundancy | 21 | 19.6 | 15.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 298 | 12.5% PEG 20000, 100 mM MES |