4TM1
Kutzneria sp. 744 ornithine N-hydroxylase, KtzI-FADred-NADP+-Br
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-04-13 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 81.888, 151.711, 162.388 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.902 - 2.390 |
R-factor | 0.2001 |
Rwork | 0.199 |
R-free | 0.22220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3s5w |
RMSD bond length | 0.009 |
RMSD bond angle | 1.289 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.430 |
High resolution limit [Å] | 2.390 | 2.390 |
Number of reflections | 78161 | |
<I/σ(I)> | 14.7 | 2.4 |
Completeness [%] | 96.8 | 98.1 |
Redundancy | 5.5 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 1.2-1.4 M sodium bromide, 22-25% PEG 3350, 0.1 M Bis-tris propane pH 7.5 |