4TLC

Crystal structure of N-terminal C1 domain of KaiC

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	100
Detector technology	CCD
Collection date	2012-01-23
Detector	RAYONIX MX225HE
Wavelength(s)	0.9
Spacegroup name	P 21 21 21
Unit cell lengths	79.880, 133.378, 149.584
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.297 - 2.090
R-factor	0.1761
Rwork	0.174
R-free	0.21870
RMSD bond length	0.003
RMSD bond angle	0.824
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.090
Number of reflections	94429
<I/σ(I)>	39.1
Completeness [%]	99.4
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293.15	PEG 400, PEG 8000