4RYK
Crystal structure of a putative transcriptional regulator from Listeria monocytogenes EGD-e
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-21 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.97872 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 86.310, 103.930, 112.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.400 - 2.090 |
R-factor | 0.1694 |
Rwork | 0.168 |
R-free | 0.19919 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.647 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.400 | 2.140 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.040 | 0.658 |
Number of reflections | 30178 | |
<I/σ(I)> | 27.1 | 3 |
Completeness [%] | 99.4 | 98.1 |
Redundancy | 7.4 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 1.1 M Ammonium Tartrate, 25 % Sucrose, 10 % PEG 400, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |