4RVQ
PWI-like domain of Chaetomium thermophilum Brr2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-25 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.91841 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 123.846, 45.752, 27.420 |
Unit cell angles | 90.00, 102.56, 90.00 |
Refinement procedure
Resolution | 26.764 - 1.135 |
R-factor | 0.1254 |
Rwork | 0.124 |
R-free | 0.14580 |
Structure solution method | SAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.477 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.790 | 1.200 |
High resolution limit [Å] | 1.135 | 1.140 |
Number of reflections | 54190 | |
<I/σ(I)> | 13 | 2.9 |
Completeness [%] | 100.0 | 92.8 |
Redundancy | 3.5 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | 2 M ammonium sulfate, 0.1 M Tris-HCl, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
2 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 1.9 M ammonium sulfate, 0.1 M Tris-HCl, 0.01 M Cobalt chloride, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |