4RS5
Crystal structure of an uncoating intermediate of a EV71 recombinant virus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2013-11-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.281579 |
Spacegroup name | P 42 3 2 |
Unit cell lengths | 350.155, 350.155, 350.155 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.791 - 3.805 |
R-factor | 0.2714 |
Rwork | 0.271 |
R-free | 0.29940 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.981 |
RMSD bond angle | 0.005 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.791 | 3.940 |
High resolution limit [Å] | 3.805 | 3.800 |
Number of reflections | 97564 | |
Completeness [%] | 81.9 | 94 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 290 | 0.1M MES containing 1.6M sodium acetate, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 290K |