4RQP
Crystal structure of the natually occurring empty particle of a clinical C4 strain EV71
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2010-10-02 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.97916 |
Spacegroup name | P 42 3 2 |
Unit cell lengths | 352.975, 352.975, 352.975 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.918 - 3.151 |
R-factor | 0.2169 |
Rwork | 0.216 |
R-free | 0.23360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.897 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.918 | 3.200 |
High resolution limit [Å] | 3.151 | 3.150 |
Rmerge | 0.904 | |
Number of reflections | 190018 | |
Completeness [%] | 90.9 | 89.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 0.1M Imidazole,1.0M sodium acetate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |