4RPD
Crystal Structure of P Domain of 485 Norovirus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97924 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 99.410, 73.500, 81.810 |
Unit cell angles | 90.00, 94.11, 90.00 |
Refinement procedure
Resolution | 48.840 - 1.510 |
Rwork | 0.146 |
R-free | 0.18700 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.009 |
RMSD bond angle | 1.286 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1690)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.840 |
High resolution limit [Å] | 1.500 |
Rmerge | 0.065 |
Number of reflections | 92638 |
<I/σ(I)> | 14.24 |
Completeness [%] | 98.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 291 | Potassium Formate 0.2 M, 20% w/v PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 18K, temperature 291K |