4RM9
Crystal structure of human ezrin in space group C2221
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.954 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 67.433, 113.517, 111.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.236 - 2.000 |
R-factor | 0.2117 |
Rwork | 0.209 |
R-free | 0.25920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2i1j |
RMSD bond length | 0.003 |
RMSD bond angle | 0.735 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.3_473)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.970 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.118 | 0.809 |
Number of reflections | 28759 | |
<I/σ(I)> | 14.1 | 3.7 |
Completeness [%] | 98.3 | 97.7 |
Redundancy | 14 | 14.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 0.1M Bis-Tris pH 5.5, 18% PEG3350, VAPOR DIFFUSION, HANGING DROP, temperature 298K |