4RKY
Crystal structure of DJ-1 isoform X1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2005-07-02 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 74.912, 74.912, 75.144 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.540 - 1.500 |
R-factor | 0.17138 |
Rwork | 0.170 |
R-free | 0.19253 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1p5f |
RMSD bond length | 0.004 |
RMSD bond angle | 0.967 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.993 | |
High resolution limit [Å] | 1.497 | 1.497 |
Number of reflections | 25856 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | 298 | 28-32% PEG400, 100 mM citrate, pH 4.6, VAPOR DIFFUSION, temperature 298K |