4RHD
DNA Duplex with Novel ZP Base Pair
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2013-12-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 3 |
Unit cell lengths | 59.429, 59.429, 87.048 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 87.050 - 1.700 |
R-factor | 0.22361 |
Rwork | 0.223 |
R-free | 0.22649 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 3.198 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 87.050 |
High resolution limit [Å] | 1.700 |
Number of reflections | 37630 |
Completeness [%] | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 10% (v/v) MPD, 40 mM Sodium cacodylate, 12 mM Spermine tetra-HCl, pH 6.0, 80 mM NaCl, 20 mM MgCl2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |