4RHB
Crystal structure of the lipopolysaccharide assembly complex LptD-LptE from the Escherichia coli outer membrane
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-E |
| Synchrotron site | APS |
| Beamline | 24-ID-E |
| Detector technology | PIXEL |
| Collection date | 2013-12-12 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.979200 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 128.040, 136.620, 108.310 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 108.310 - 3.355 |
| R-factor | 0.2606 |
| Rwork | 0.257 |
| R-free | 0.33780 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4q35 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.437 |
| Refinement software | REFMAC (5.8.0071) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 200.000 |
| High resolution limit [Å] | 3.355 |
| Number of reflections | 26835 |
| Completeness [%] | 96.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
