4RGD
The structure a AS-48 G13K/L40K mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.820, 49.910, 41.720 |
Unit cell angles | 90.00, 98.16, 90.00 |
Refinement procedure
Resolution | 24.100 - 1.200 |
R-factor | 0.11969 |
Rwork | 0.118 |
R-free | 0.14704 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o82 |
RMSD bond length | 0.021 |
RMSD bond angle | 2.039 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.900 | 1.220 |
High resolution limit [Å] | 1.200 | 1.200 |
Number of reflections | 41746 | |
Completeness [%] | 100.0 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 295 | 0.2 M ammonium acetate, 30% PEG4K, 0.1M sodium citrate tribasic dihydrate plus ANAPOE-58, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 295K |